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Crystal Structure Determination from Experimental Powder Data
The Powder Solve method, available within from Accelrys, allows the determination of crystal structures of complex molecular solids directly from high-quality experimental powder diffraction data. Here are the Powder Solve results for cimetidine. On the left is the comparison of powder patterns...
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Crystal Structure Determination from Conventional Powder Diffraction Data: Application to Hydrates, Hydrochloride Salts, and Metastable Polymorphs
The Powder Solve method, available within Accelrys' product, has been used by Gregory A. Stephenson at Eli Lilly to re-determine the crystal structures of papaverine hydrochloride and erythromycin A dihydrate, and to solve the crystal structure of the metastable polymorph B of acetohexamide [1...
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Determination of Volume Percent Retained Austenite by X-Ray Diffraction (.pdf)
that is dependent. upon the selection of instrumentation. EXAMPLES. geometry and radiation but independent of. the sample. R depends upon the interplanar. Figures 1 and 2 show examples of retained. spacing, the Bragg angle, crystal structure. austenite distributions as functions of depth. A. and composition...
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X-ray Diffraction Residual Stress Techniques (.pdf)
determination at their. dimensions of the crystals. Microstresses vary from point. current state of development. In addition, their spatial and. to point within the crystal lattice, altering the lattice. depth resolutions are orders of magnitude less than those. spacing and broadening...
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PAT Brings Laboratory Analysis Online
response times to process upsets and often eliminating the need for sampling altogether. Here, then, a sampling of recent PAT tools for the pharmaceutical manufacturing marketplace. Crystal Size and Shape in Real Time Crystal Scope is an online PAT tool designed to help optimize processes...
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Femtosecond Verses Nanosecond Laser Machining: Comparison of Induced Stress and Structural Changes in Silicon
durations in the nanosecond (NS) regime. In this paper, we compare the results of micromachining a single crystal silicon wafer using a 150-femtosecond and a 30-nanosecond lasers. doi:10.1016/j.apsusc.2004.08.029 Applied Surface Science 242 (2005) 162167. www.elsevier.com/locate/apsusc...
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Beta testing an in-line monitor for moisture measurement in inert gas lines
was described in an earlier issue of Designed to measure moisture levels in ultra-high-purity (UHP) nitrogen and argon gases, the monitor uses a piezoelectric quartz crystal microbalance (QCM) sensor. The quartz crystal is coated with a thin film of barium metal, with which moisture reacts irreversibly...
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The Uniformity Of Shot Peening Induced Residual Stress (.pdf)
info@lambdatechs.com Ph: (513) 561-0883 Toll Free/US: (800) 883-0851. Lambda Technologies. www.lambdatechs.com info@lambdatechs.com. TABLE I. TECHNIQUE. SAMPLE MATERIAL AND PROPERTIES. Determination of Single Crystal Elastic. ASTM SA 508 Class 2 Pressure Vessel Steel. Constants. Nominal Composition (%...
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Smart and small
, the wire is usually prestrained up to 5% in its more malleable low-temperature state. The amount of prestrain and the wire's length determine the actuator's stroke. When heated above its transition temperature, the material's crystal structure shifts into a higher-stiffness form, contracting...
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PAT and the Crystallization Toolkit
crystal product. This can be greatly facilitated by measurement of important crystallization characteristics such as the crystal size and the liquid phase concentration over the course of a batch. Ideally, these measurements should be made so as to avoid the inherent difficulties associated...