Chemical Process Equipment: Selection and Design, Second Edition

Chapter 11: Solid-Liquid Separation

Solid-liquid separation is concerned with mechanical processes for the separation of liquids and finely divided insoluble solids

11.1. PROCESSES AND EQUIPMENT

Solid-liquid is not usually considered a "high-tech" operation. Much equipment for the separation of liquids and finely divided solids was invented independently in a number of industries and is of diverse character. These developments have occurred without benefit of any but the most general theoretical considerations. Even at present, the selection of equipment for specific solid-liquid separation applications is largely a process of scale-up based on direct experimentation with the process material.

The nature and sizing of equipment depends on the economic values and proportions of the phases as well as certain physical properties that influence relative movements of liquids and particles. Pressure often is the main operating variable so its effect on physical properties should be known. Table 11.1 is a broad classification of mechanical processes of solid-liquid separation. Clarification is the removal of small amounts of worthless solids from a valuable liquid. Filtration is applied to the recovery of valuable solids from slurries. Expression is the removal of relatively small contents of liquids from compressible sludges by mechanical means.

Table 11.1: Chief Mechanical Means of Solid-Liquid Separation

1.

Settling

a.

by gravity

i.

in thickeners

ii.

in classifiers

b.

by centrifugal force

c.

by air flotation

d.

by dense media flotation

e.

by magnetic properties

2.

Filtration

a.

on screens, by gravity

b.

on filters

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