From Water Contamination Emergencies: Can We Cope?
Dstl, Porton Down, Salisbury Crown Copyright 2003 Dstl
1 INTRODUCTION
Current analytical methods used in the water industry for compliance monitoring are not well suited to detection of water contamination during emergencies. This applies to early warning of harmful chemical releases as well as the presence of biological contamination (which can take days rather than hours or minutes to provide a definitive result). A case is therefore made for improved rapid methods of analysis to meet this important requirement. Consideration is given to the relative merits of targeted analysis versus screening techniques, with examples provided. One approach to targeted analysis of organic contaminants is to optimise the performance of chromatographic separation and identification techniques. An alternative is to screen using a spectroscopic method such as UV absorption or Surface Enhanced Raman Spectroscopy (SERS), both of which involve minimal sample handling and have potential for at site use. Other potentially useful techniques for rapid screening for chemical and microbiological contaminants are also listed, some of which are described in greater detail in subsequent chapters. In conclusion, it is argued that targeted and screening techniques both have a role to play in contamination monitoring; using targeted analysis with optimised methodology for identification, combined with screening techniques in order to prioritise suspect samples for targeted analysis.
It may at times be appropriate to operate both of these methods in parallel to meet tight deadlines involved in providing timely information to decision-makers. Selecting the required methodology and analytical capabilities will depend on...
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Topics of Interest
2 CURRENT METHODS OF ANALYSIS Methods of analysis in routine use within the water industry are geared primarily to compliance with UK Drinking Water Regulations. [1] This predicates use of validated...
8 SCREENING VS TARGETED ANALYSIS Screening and rapid target analysis both have a role to play in water contamination emergencies. Targeted analysis requires development of rapid methods optimised for...
A host of field-screening methodologies — including immunoassay and turbidimetric techniques, field-hardened infrared spectroscopy and gas chromatography, and the use of organic vapor analyzers...
6 SCREENING TECHNIQUES Screening techniques are useful as a first level of testing. However most lack the discriminating power and reliability of targeted methods. A number of possible approaches are...
Visible and near-infrared (NIR) spectra and samples for laboratory microbial analysis were acquired of fecal contaminants, ingesta contaminants, and bare processing equipment surfaces (rubber and...