Rules of Thumb for Chemical Engineers: A Manual of Quick, Accurate Solutions to Everyday Process Engineering Problems, Fourth Edition

Chapter 8: Separators/Accumulators

Liquid Residence Time

For vapor/liquid separators there is often a liquid residence (holdup) time required for process surge. Tables 1, 2, and 3 give various rules of thumb for approximate work. The vessel design method in this chapter under the Vapor/Liquid Calculation Method heading blends the required liquid surge with the required vapor space to obtain the total separator volume. Finally, a check is made to see if the provided liquid surge allows time for any entrained water to settle.

Table 1: Residence Time for Liquids

Service (times in minutes)

Full (Reference 1 )

L HL to L LL (minimum) Reference 2 [*] )

Full (Reference 3 )

Miscellaneous

Tower reflux drum

See Table 2

5-based on reflux flow

5 to 10-based on total flow

Vapor-liquid separators

3 5

Product to storage

Depends on situation

Fractionator O.H. Prod. 2

Product to heat exchanger along with other streams

Fractionator O.H. Prod. 5

Product to heater

Fractionator O.H. Prod. 10

Furnace surge drums

10 min.

20 max.

Tower bottoms

5 min.

  • FRC control

10 max.

  • LC control

3 min.

[*] This article deals only with reflux drums. Use only the larger vessel volume determined. Do not add two volumes such as reflux plus product. If a second liquid phase is to be settled, additional time is needed. For water in hydrocarbons, an additional 5 minutes is recommended.

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