Handbook of Adhesives and Sealants

Appendix D: Surface Preparation Methods for Common Substrate Materials

D.1 Surface Preparation Methods for Metal Substrates

Substrates

Cleaning solvents

Substrate treatments

Comments

Aluminum and aluminum alloys

Trichloroethylene

1. Sandblast or 100 grit emery cloth followed by solvent degreasing

Medium to high strength bonds, suitable for non critical applications

2. Immerse for 10 min at 70 82 C in a commercial alkaline cleaner or

Optimum bond strength per FPL etch process. Specified in ASTM D 2651 and MIL-A-9067. Solvent degrease may replace alkaline cleaning

  • Sodium metasilicate

3.0

  • Sodium hydroxide

1.5

  • Sodium dodecylbenzene sulfonate, such as

    • Nacconol 90G (Stephan Co., Nothfield, IL)

1.5

  • Water (distilled)

128.0

Wash in water below 65 C and etch for 12 15 min at 66 71 C in

  • Sodium dichromate

1.0

  • Sulfuric acid (96%)

10.0

  • Water (distilled)

30.0

Rinse in distilled water after washing in tap water and dry in air

3. Alkaline clean as described in 2 above. Then immerse for 10 12 mins at 60 65 C in the following solution:

P-2 etch specified in ASTM D 2651

  • Sulfuric acid (6.5 to 9.5N)

7 36% by wt.

  • Ferric sulfate

135 to 165 g/l

Rinse as descirbed in 2 above

4. Degrease with solvent. Abrade lightly with mildly abrasive cleaner. Rinse in deionized water; wipe; or air dry. Etch 20 min at RT in

Room temperature etch

  • Sodium dichromate

2

  • Sulfuric acid (96%)

7

Rinse thoroughly in deionized water; dry at 70 C for 30 min

5. Form a paste using sulfuric acid sodium dichromate solution and finely divided silica or fuller's earth. Apply; do not permit paste to...

UNLIMITED FREE
ACCESS
TO THE WORLD'S BEST IDEAS

SUBMIT
Already a GlobalSpec user? Log in.

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.

Customize Your GlobalSpec Experience

Category: Cleaning Agents and Surface Treatments
Finish!
Privacy Policy

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.