Flow Measurement

Chapter 27 - Laboratory Primary Standards

Meter manufacturers and users utilize laboratories with primary flow standards
to calibrate their working flowmeter standards. Such laboratory standards are
designed to have the lowest practical measurement uncertainty so that this high
accuracy can be passed on to the flowmeter being calibrated and subsequently to
the flowmeter application. Laboratory standards are used to assess flowmeter performance
under ideal conditions (generally field performance is not as good).
Presently, the uncertainty of laboratory standards is reported to be typically less
than 0.2% with a 95% level of confidence. All of the uncertainties herein will be
expressed as 95% level of confidence values unless otherwise stated. Laboratory
flow standards exist for liquid flows from approximately 0.1 g/min to 10,000 kg/
min and for gas flows from approximately 1x10-6 g/min to 100 kg/min. The low
uncertainty requirement generally means that these devices are used in tightly
controlled laboratory environments and are not portable. Laboratory flow standards
can be grouped into certain general categories, and examining their principles
and methods of operation is useful for those seeking to establish a flow
calibration laboratory or understand the laboratory calibration process. Laboratory
standards are typically custom-built devices, unique in design, but some commercially-
built laboratory standards are available.

Primary Standards

A primary standard is defined as a device or object used as the reference in a
calibration that is acknowledged to be of the highest meteorological quality and
that derives its measurement without reference to some other standard of the same
quantity (Ref. 1). For example, a flowmeter that has been calibrated against a flow
standard and is subsequently used to calibrate other flowmeters is not a primary
standard (it is a reference standard or transfer standard). A piston prover that has
had all of the necessary lengths as well as its pressure, temperature, and time
instrumentation calibrated can be a primary standard. It is desirable that the
calibrations necessary for the primary standard be based on fundamental measurands
(time, length, temperature, etc.) and not on some more complex derived quantities.
It is important that the primary standard be compared to other primary standards
to establish that it is working properly and to verify its uncertainty
specifications. Other important characteristics of a primary standard are a well- established theory of operation or basis equation and a detailed uncertainty analysis.
The uncertainty analysis is critical to assessing the uncertainty of the flowmeter
calibrations performed with the primary standard. It is helpful if a primary
standard is conceptually simple and its proper operation easy to verify since it is
often the arbiter of flow measurement disputes.

A primary standard is
defined as a device or
object used as the
reference in a calibration that is acknowledged to
be of the highest
meteorological quality
and that derives its
measurement without
reference to some other standard of the same quantity (Ref. 1).

 

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